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Several metal–organic frameworks of nickel(II) were obtained starting from the molecular complex 1, [Ni(OH2)4(4‐pyc)2] (4‐pyc = 4‐pyridinecarboxylate or isonicotinate). By using different reaction conditions, two polymorphs of the anhydrous complex [Ni(4‐pyc)2]n (2a and 2b) and the polynuclear compound [Ni5(OH2)3(4‐pyc)10]n (3) were obtained in very high yield. All of the compounds were characterized...
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