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CsCl‐type intermetallic compounds TiM (M=Co, Fe) were obtained by deoxidizing trigonal ilmenite‐type MTiO3 with a reducing agent CaH2 in molten LiCl at 600 °C. X‐ray diffraction, nitrogen adsorption, scanning electron microscopy, and transmission electron microscopy with energy‐dispersive X‐ray, and X‐ray photoelectron spectroscopy analyses revealed the formation of nanoscale layered structures, which...