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Materials derived from surface‐mounted metal–organic frameworks (SURMOFs) are promising electrocatalysts for the oxygen evolution reaction (OER). A series of mixed‐metal, heterostructured SURMOFs is fabricated by the facile layer‐by‐layer deposition method. The obtained materials reveal record‐high electrocatalyst mass activities of ≈2.90 kA g−1 at an overpotential of 300 mV in 0.1 m KOH, superior...
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