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Using 4‐connected pyrene‐based building blocks with D2h symmetry and 2‐connected fluorene‐based linker with C2v symmetry, a 2D porous organic framework is obtained via imine condensation, PAF‐130. PAF‐130 has high crystallinity, permanent, and a high photoluminescence quantum yield, which is as high as 29.5% when dispersed in acetonitrile.
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