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A thermostable anion-pillared metal-organic framework TIFSIX-2-Ni-i (also referred to as ZU-12-Ni, TIFSIX = hexafluorotitanate, 2 = 4,4′-bipyridylacetylene, i = interpenetrated) has been synthesized for the first time. Structural characterizations show that TIFSIX-2-Ni-i exhibits a 2-fold interpenetrated network with narrow aperture of 5.1 Å (H-H distance) and abundant inorganic anion sites in the...
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