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Engineering sophisticated structure of Al2O3 and controlling the structure of counterpart metal active sites remain challenges to achieve a high catalytic‐performance in heterogeneous catalysis. Herein, we present a confinement strategy to stabilize homogeneous Ni by penta‐coordinated Al3+ anchoring sites in Al2O3. This approach is involved in using a metal–organic framework as host to load Ni2+ ions,...
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