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Acetylene purification from methane is challenging in the field of porous organic polymers (POPs). Herein, we have provided one‐pot Ullmann coupling reaction to synthesize a series of POPs with rich N‐sites, named FJU‐POP‐n, wherein the low‐cost and non‐toxic Cu(acac)2 and environmental‐friendly glycerol are employed as catalyst and solvent, respectively. These POPs constructed by aromatic amine and...
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