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A new sextet ground state molecule, the 2,4,6‐trichloro‐1,3‐dinitrenophenoxyl radical, was obtained upon UV photolysis of the corresponding diazido precursor in argon at 5 K. The sextet molecule is formed stepwise with the triplet nitrene, the quartet nitreno radical, and the quintet dinitrene as intermediates that were detected by EPR spectroscopy. IR and UV–Vis measurements only allowed us to observe...
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