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The aggregation behavior of an amphiphilic copper(II) complex was studied in solution by means of UV‐Vis and EPR spectroscopy. While dilute solutions in polar media do not give indication of relevant intermolecular interactions, concentrated solutions in nonpolar media clearly do not reflect the molecular properties of [CuL] (H2L: N2O2 ligand of the Jäger‐type with bulky head‐group and long alkoxy...
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