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Well‐defined palladium trigonal bipyramidal/tetrahedral nanocrystals were synthesized by an aqueous‐phase hydrothermal method. The final products were a mixture of trigonal bipyramidal and tetrahedral nanocrystals. Statistics indicated that there were more trigonal bipyramids than tetrahedra in the products. Ethylenediamine tetraacetic acid disodium salt (EDTA‐2Na) was proven to be essential in controlling...
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