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A visible light photosensitizing metal‐organic cage is applied as an artificial supramolecular reactor to control the reaction of aryl radicals with terminal olefins under green light/solvent conditions, which facilitates selective transformation in the confined enzyme‐mimicking environment to give a series of geometrically defined E/Z‐alkenes. The hydrophobic cage displays good host–guest inclusion...
A visible light photosensitizing metal‐organic cage is applied as an artificial supramolecular reactor to control the reaction of aryl radicals with terminal olefins under green light/solvent conditions, which facilitates selective transformation in the confined enzyme‐mimicking environment to give a series of geometrically defined E/Z‐alkenes. The hydrophobic cage displays good host–guest inclusion...