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Multifunctional theranostic agents have become rather attractive to realize image‐guided combination cancer therapy. Herein, a novel method is developed to synthesize Bi2Se3 nanosheets decorated with mono‐dispersed FeSe2 nanoparticles (FeSe2/Bi2Se3) for tetra‐modal image‐guided combined photothermal and radiation tumor therapy. Interestingly, upon addition of Bi(NO3)3, pre‐made FeSe2 nanoparticles...
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