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High energy ball milling (HEBM) with ZrO 2 balls is shown to be an efficient method for the preparation of silicon nanocrystals (SiNCs), which exhibit excellent photocatalytic activity for the reduction of CO 2 in aqueous solution. TEM indicated that the size of the as-prepared SiNCs ranged from 1 to 4nm, and XRD data confirmed that the crystallinity of the SiNCs was well preserved...
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