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New rare earth iodide carbodiimide nitride compounds with the composition RE2I(CN2)N (RE = La, Gd) were successfully synthesized by multilateral solid‐state metathesis reaction from RE triiodides, LiN and Li2(CN2). The crystal structures of RE2I(CN2)N were refined from X‐ray powder diffraction data with the space group Cmmm. LaI(CN2) was prepared from a mixture of LaI3 and Li2(CN2). The crystal structure...
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