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The structure of {HC(3,5-Me 2 pz) 3 Fe[μ-p-C 6 H 4 (CH 2 OCH 2 C(pz) 3 ) 2 ]Fe(3,5-Me 2 pz) 3 CH}(BF 4 ) 4 (pz=pyrazolyl ring) contains two octahedral iron(II) centers linked by a semirigid, bitopic tris(pyrazolyl)methane ligand. The solid-state structure shows the two heteroleptic-bonded iron(II) centers...
The synthesis, structural, magnetic, and Mössbauer spectral properties of Fe[(C 6 H 5 )B(3-Mepz) 3 ] 2 (2, pz=pyrazolyl ring) are reported. The single crystal X-ray structural results indicate that at both 294 and 90K Fe[(C 6 H 5 )B(3-Mepz) 3 ] 2 (2) has a distorted octahedral iron(II) coordination environment with Fe–N bond distances...
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