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Two dinuclear complexes with Cu···Cu distances above 7 Å were characterized by X‐ray diffraction, EPR spectroscopy, solution speciation, and cyclic voltammetry. Both complexes display EPR spectra typical of dipole–dipole‐coupled dicopper(II) complexes. The two complexes presented herein are part of a series of dinuclear complexes with catecholase activity, and they exhibit the highest catalytic efficiencies...
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