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Metal–organic frameworks (MOFs) with expanding porosity and tailored pore environments are intriguing for catalytic applications. We report herein a straightforward method of controlled partial linker thermolysis to introduce desirable mesopores into mono‐ligand MOFs, which is different from the classical thermolyzing method that starts from mixed‐linker MOFs. UiO‐66‐NH2, after partial ligand thermolysis,...
Metal–organic frameworks (MOFs) with expanding porosity and tailored pore environments are intriguing for catalytic applications. We report herein a straightforward method of controlled partial linker thermolysis to introduce desirable mesopores into mono‐ligand MOFs, which is different from the classical thermolyzing method that starts from mixed‐linker MOFs. UiO‐66‐NH2, after partial ligand thermolysis,...