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Fine powders of pure Si2N2O were SHS-produced under pressure of nitrogen gas from mixtures doped with FeCl3 · 6H2O, and the influence of process conditions was explored by XRD and SEM/EDS. Pure 2D-nanopowders of Si2N2O were obtained in the presence of 15 × 10–3 M FeCl3 · 6H2O in green 3Si + SiO2 mixture at P(N2) = 5 MPa.
The effect of iron-containing catalysts–FeCl3 · 6H2O, Fe2(C2O4)3 · 5H2O, and Fe(NO3)3 · 9H2O–on phase composition, morphology, and particle size of products formed upon combustion of Si–C mixtures in nitrogen gas. Composition and granulometry of combustion products were found to depend on a type and amount of the above additives to green composition. The results may turn interesting for researchers...
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