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We carried out covalent functionalization of single‐ and double‐walled carbon nanotubes (SWNTs and DWNTs) comparatively by using isocyanate chemistry. The introduction of aromatic diisocyanate on the sidewalls of the tubes was verified by the strong IR peak around 2272 cm–1 arising from the NCO asymmetric stretching mode, by the intensified sp3 peak at 285.2 eV in the C1s photoemission spectra, and...
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