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In this paper, we use cyclic voltammetry to investigate the effect of protons on the conductivity and reactivity of TiO2 nanotube array (NTA) electrodes in an aqueous redox system. The H+ ion can change the TiO2 nanotube (anatase phase) surface states for electrons transfer. It can also act as an intermediate state for electron transfer to the acceptor species in the electrolyte surrounding the TiO...
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