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It's just a phase: A highly fluorinated compound with a rigid three‐dimensional architecture was synthesized as a monomer for poly(p‐phenyleneethynylene)s (PPEs). Fluorous biphase reactions were applied for the synthesis of a PPE that is soluble only in fluorous solvents. A fluorous solution of the polymer could be processed into aqueous emulsions that display high fluorescence quantum yields (see...
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