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Fluorographites (CFx) are ultrahigh‐energy‐density cathode materials for alkaline‐metal primary batteries. However, they are generally not rechargeable. To elucidate the reaction mechanism of CFx cathodes, in situ transmission electron microscopy characterizations and ab initio calculations are employed. It is found that it is a two‐phase mechanism upon K/Na/Li ion insertion; crystalline KF (crystalline...
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