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Using phosphoric acid as the catalyst and glucose as substrate, microwave-assisted solid-phase oligosaccharide synthesis was studied. The parameters were optimized by orthogonal test design and statistical analysis method. Under the optimum reaction conditions, namely microwave power output of 1000W, microwave irradiation time 9min, adding 30% water to initiate reaction, adding 4% heteropoly acid...
Using phosphoric acid as the catalyst and glucose as substrate, microwave-assisted solid-phase bioactive oligosaccharide synthesis was studied. The optimum reaction conditions were that microwave power output of 800W, microwave irradiation time 10min, adding 30% water to initiate reaction, adding 10% heteropoly acid A as the catalyst. The yield ratio of product was 76.56%. The product was characterized...
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