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A general and simple strategy is realized for the first time for the preparation of metal sulfide (MxSy) nanoparticles immobilized into N/S co‐doped carbon (NSC) through a one‐step pyrolysis method. The organic ligand 1,5‐naphthalenedisulfonic acid in the metal–organic framework (MOF) precursor is used as a sulfur source, and metal ions are sulfurized in situ to form MxSy nanoparticles, resulting...
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