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The results of a complete thermogravimetric study of copper benzene-1,3,5-tricarboxylate (Cu-BTC or HKUST-1) are reported here together with mass spectrometry (MS) and Fourier transform infrared spectroscopy (FTIR) analyses of the evolved gases up to 800°C. Oxidative and inert conditions were applied to reveal the stoichiometry of the as-received synthesis product. In spite of using a water-ethanol...
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