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A hydrothermal-based synthesis technique was used to produce both amorphous and nano-grained NiO nanowires. The scanning electron microscopy images showed the morphologies before and after annealing treatment at 350 and 400°C for 2h. The microstructural features of the mixed amorphous and local crystalline in as-synthesized NiO and polycrystalline in annealed NiO were characterized by X-ray diffraction,...
Nanorods (NRs) with square-cross-sections, sword-like NRs, and nanowires (NWs) of SnOx were synthesized by catalyst-free thermal evaporation of Sn powder in the presence of O2 gas. The effects of synthesis temperature on the morphology and photoluminescence are presented. Although it is possible that different growth mechanisms occurs simultaneously in this narrow temperature zone, predominant morphologies...
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