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The radical polymerization of styrene initiated with tetraethylthiuram disulfide (TD)/nickel (II) chloride (NiCl 2 )/triphenylphosphine (PPh 3 ) was of living nature via a one-electron redox reaction between nickel(II) and (III) species. The mechanism belonged to reverse atom transfer radical polymerization (reverse ATRP). The living essence was affected by the molar concentration...
A facile method for synthesis of well-defined ABA triblock copolymers, such as poly(vinyl acetate-b-styrene-b-vinyl acetate), was investigated. The polymerization proceeds ‘living’ radical mechanism realized by macro-iniferter technique. The macro-iniferters were designed and synthesized by ‘living’ radical polymerization of vinyl monomers utilizing diethyl 2,3-dicyano-2,3-di(p-N,N-diethyldithiocarbamymethyl)phenylsuccinate...
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