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Finely divided polymer-stabilized PdZn bimetallic nanoclusters are prepared by the polyol method. TiO2 matrix-impregnated nanoclusters coated on the inner surface of a capillary microreactor are used as catalysts for the selective hydrogenation of 2-methyl-3-butyn-2-ol. The effect of the activation conditions (duration, temperature, and gas medium composition) on the physicochemical and catalytic...
A continuously working capillary microreactor with a catalytic coating based on mesoporous titanium dioxide with embedded Pd nanoparticles was tested in a reaction of the selective hydrogenation of 2-methyl-3-butyn-2-ol (MBI). The catalytic coatings were obtained by the supporting of a carrier sol, which contained colloidal Pd nanoparticles, onto the internal wall of a quartz capillary with a diameter...
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