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The complex [Pt(9S3)(SbPh 3 )(Ph)](PF 6 ) forms directly from [Pt(9S3)(SbPh 3 ) 2 ](PF 6 ) 2 during the room temperature crystallization of the latter in nitromethane. The crystal structure shows a five-coordinate Pt(II) center containing the tridentate thiacrown ligand, a Sb donor from the triphenylstibine ligand, and a σ-coordinating phenyl group....
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