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Pulsed base (OH−) electrogeneration was applied to the cathodic electrodeposition of manganese oxide from chloride bath for the first time, and Mn3O4 nanorods were prepared. The deposition experiments were performed under a pulse current mode in a typical on-times and off-times (ton=10ms and toff=50ms) at a peak current density of 1mAcm−2 (Ia=1mAcm−2). The structural characterizations with XRD and...
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