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Synthesis of high‐purity high‐entropy metal diboride powders is critical to implementing their extensive applications. However, the related studies are rarely reported. Herein we first theoretically studied the synthesis possibility of high‐purity high‐entropy diboride powders, namely (Hf0.25Ta0.25Nb0.25Ti0.25)B2 (HTNTB), via boro/carbothermal reduction by analyzing the thermodynamics of the possible...
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