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The kinetic behavior of bis(2‐methyl) butylene carbonate (BMBC) by the transesterification of dimethyl carbonate (DMC) with 1,4‐butanediol (BDO) was investigated experimentally and theoretically. The Fourier transform infrared spectroscopy (FTIRs) test confirmed that the BMBC was successfully synthesized. The optimum preparation process of BMBC was investigated at atmospheric pressure, where Zn(Ac)...