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Two organotin complexes of two types were synthesized by different methods basing on the same materials. Characterizations of the complexes were achieved by elemental analysis, IR, NMR ( 1 H, 13 C and 119 Sn) spectroscopy and X-ray crystallography diffraction analysis. X-ray data reveal that complex 1 is an 8-membered cycle and complex 2 is a surprising mixed sodium organotin...
Treatment of a suspension of AgNO 3 and AgCl in MeOH with a solution of N,N,N′,N′-tetra(diphenylphosphanylmethyl)ethylene diamine (dppeda) in CHCl 3 afforded a binuclear complex [Ag 2 (dppeda)Cl](NO 3 )·2MeOH (1). The analogous reactions using AgSCN and dppeda in EtOH/CH 2 Cl 2 gave rise to a polymeric complex [Ag 2 (dppeda)(SCN) 2 ]...
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