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A variety of organotin triflate clusters are obtained by treating dialkyltin oxide with triflic acid (TfOH) in different ratios. When R 2 SnO is exposed to 0.5 equivalents of TfOH, 3-hydroxy-1-triflato distannoxanes (1) are formed which have a novel sheet-like structure in the solid state. Treatment of R 2 SnO with 2/3 or one equivalent of TfOH affords a trinuclear cluster 3 or cationic...
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