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In acetonitrile and tetrahydrofuran solutions, irradiation of [ReBr 6 ] 2− leads to the replacement of a bromide by a solvent molecule, followed at a much slower rate by the photosolvation of a second bromide. The quantum yield for the primary photosolvation is 0.013 in CH 3 CN. As an alternative to photolysis occurring through a doublet d–d excited state, it is suggested that...
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