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We report NiII and CuII complexes of a few pyrrolecarboxamide ligands containing –H, –Cl, and –CH3 substituents on the phenylene ring. Solid‐state X‐ray diffraction and solution‐based spectral studies substantiated a square‐planar geometry around the metal ions in all six of the MII complexes. Electrochemical studies showed that the electronic substituents considerably influence the M3+/2+ redox potentials...
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