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Experiments involving single step hydrothermal reactions of the divalent metal (Zn2 + , Cd2 + , Pb2 + , Cu2 + , Ni2 + and Mn2 + ) salts with ilmenite NaSbO3 yielded pure divalent antimonates in the case of CdSb2O6 crystallizing in the PbSb2O6 type structure and ZnSb2O6 crystallizing in the trirutile structure type. In the case of Pb2 + , Cu2 + , Ni2 + and Mn2 + divalent cations, phase pure product...
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