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A novel solvothermal oxidation route has been used to prepare hydroxyl-free nanocrystalline zinc oxide via the oxidation of zinc powder with trimethylamine N-oxide (Me 3 N→O) or 4-picoline N-oxide (4-picN→O) in different organic solvents under dry nitrogen atmosphere. It is found that both oxygen sources and solvents have great effect on morphologies and sizes of nanocrystalline ZnO. The role...
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