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Solution combustion method was used to synthesize ZnCo2O4 nanoparticles. Then, physical blending method was used to prepare ZnCo2O4/polyaniline (PANI) composite. The crystallite sizes of the ZnCo2O4 and ZnCo2O4/PANI composites prepared were 17.16 nm and 25.46 nm, respectively, as calculated by XRD studies. The density of nanoparticles, cell parameters, and unit cell volume were calculated by Rietveld...
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