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The study of non-hydrolytic reactions for the synthesis of NASICON is reported. Different procedures have been considered, changing the precursors and their addition order, and varying the reaction solvent; dichloromethane, acetonitrile and tetrahydrofuran (THF). The most promising results in terms of homogeneous reactivity were obtained using PO(On-C4H9)3, Zr(Ot-C4H9)4, SiCl4 and Na(Ot-C4H9) in acetonitrile...
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