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Materials for high‐efficiency photocatalytic CO2 reduction are desirable for solar‐to‐carbon fuel conversion. Herein, highly dispersed nickel cobalt oxyphosphide nanoparticles (NiCoOP NPs) were confined in multichannel hollow carbon fibers (MHCFs) to construct the NiCoOP‐NPs@MHCFs catalysts for efficient CO2 photoreduction. The synthesis involves electrospinning, phosphidation, and carbonization steps...
The dinuclear Co complex [(TPA)Co(μ‐OH)(μ‐O2)Co(TPA)](ClO4)3 (1, TPA=tris(2‐pyridylmethyl)amine) catalyzes the oxidation of water. In the presence of [Ru(bpy)3]2+ and S2O82−, photoinduced oxygen evolution can be observed with a turnover frequency (TOF) of 1.4±0.1 mol(O2) mol(1)−1 s−1 and a maximal turnover number (TON) of 58±5 mol(O2) mol(1)−1. The complex is shown to act as a molecular and homogeneous...
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