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Temperature-modulated DSC TOPEM® method was applied to study amorphization in directly synthesized high-temperature polymorph of tetra-arsenic tetra-sulfide β-As4S4 affected to high-energy mechanical milling in a dry mode with 100–600 min−1 rotational speeds. The appeared amorphous phase is shown to possess dual nature, being related to As-rich glassy-like substances with low- and high-temperature...
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