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Mono‐elemental antimonene as a new member of the 2D material family has recently attracted huge attention, whereas the higher chemical activity and narrower interlayer gallery have impinged the quality of product upon exfoliation from the bulk counterpart. To overcome the intrinsic drawbacks, along with the line of the liquid‐phase exfoliation (LPE) method, here, a pressurized alloying approach introduces...
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