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The titanium hydrolysis in the concentrated titanyl sulfate solution is essential to the TiO2 production by using the new NaOH roasting method proposed by authors, which is undergoing to scale up. The experimental titanium hydrolysis was detected by the infrared and Raman spectra for the first time to reveal the significant role of SO42− ions. The bridging bidentate SO42− ligands arrange the Ti–O...
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