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AtomlagenabscheidungR. G. Gordon et al. berichten in der Zuschrift auf S. 10384 ff. über die Verwendung eines unbeständigen dimeren Calcium(II)‐Amidinat‐Komplexes als hoch effiziente ALD‐Vorstufe für die Synthese von einheitlichen CaS‐Filmen.
We have prepared two new CaII amidinates, which comprise a new class of ALD precursors. The syntheses proceed by a direct reaction between Ca metal and the amidine ligands in the presence of ammonia. Bis(N,N′‐diisopropylformamidinato)calcium(II) (1) and bis(N,N′‐diisopropylacetamidinato)calcium(II) (2) adopt dimeric structures in solution and in the solid state. X‐ray crystallography revealed asymmetry...
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