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In this study, the hydroxypropyl β‐cyclodextrin hybrid monolithic material was fabricated and firstly applied as an adsorbent for dispersive solid‐phase extraction coupled with high‐performance liquid chromatography to detect trace‐level seven fluoroquinolones in water samples. The prepared hydroxypropyl β‐cyclodextrin hybrid monolithic material was characterized by Fourier‐transform infrared spectroscopy,...