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We report here the synthesis of well-defined thermoresponsive diblock copolymer bearing amino acid diamide derivatives, poly(N-acryloyl-l-valine N′-methylamide)-b-poly(ethylene glycol) monomethylether, via click reaction using CuSO4/sodium ascorbate as catalyst in DMF/water mixed solvent. The effects of chain length and water volume fraction in DMF on coupling efficiency were investigated. For those...
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