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The highly sensitive spectroscopic ellipsometry (SE) was first employed to in situ monitor the growth of anodic ZrO 2 nanotubes in F − -containing inorganic electrolyte within the first 80s anodization. The evolution of the characteristic parameters of anodic ZrO 2 film upon anodization was obtained by deconvoluting the ellipsometric spectra with appropriate models. Four successive...
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