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An efficient electrocatalyst for oxygen evolution has been prepared via the deposition of iron–nickel layered double‐hydroxide (FeNi‐LDH) nanosheets on 3D carbon network as the building scaffold in a one‐step hydrothermal process. It is found that upon the assembling of FeNi‐LDH nanosheets with graphene into the 3D cross‐linked hybrid, the FeNi‐LDH/graphene hybrid features a well‐improved catalytic...
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