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The MgZrF6·nH2O (n = 5, 2 and 0) compounds were studied by the methods of X‐ray diffraction and 19F, MAS 19F, and 1H NMR spectroscopy. At room temperature, the compound MgZrF6·5H2O has a monoclinic C‐centered unit cell and is composed of isolated chains of edge‐sharing ZrF8 dodecahedra reinforced with MgF2(H2O)4 octahedra and uncoordinated H2O molecules and characterized by a disordered system of...
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